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The students are able to

understand and be able to apply the basic rules for occupational safety in the organic preparative laboratory;

master various techniques for the purification of organic compounds, including distillation, filtration, recrystallization, precipitation, sublimation and extraction with work-up to acidic, basic and neutral compounds;

carry out stoichiometric calculations for organic chemical reactions and use chemical databases and formula characterization programs for support.

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Safety in the organic preparative laboratory (basic rules, deactivation and disposal of reactive chemicals, general rules of conduct); materials for laboratory materials, glassware and construction of standard reaction apparatus, ground joints and screw connections; characterization of organic compounds using melting point, boiling point, refractive index and specific rotation value; basic techniques for the purification of organic compounds (distillation under various pressure conditions, filtration, recrystallization, precipitation, sublimation); Extraction with processing for acidic, basic and neutral compounds; drying of solids, solutions and solvents; special cleaning operations for absolute solvents; working with gases (reactive gases, absorption of resulting gases, protective gases); cleaning of laboratory equipment; stoichiometric calculation of organic-chemical reactions and use of chemistry-specific drawing programs, chemistry databases; selected application examples

lecture

written

Will be discussed in the first lesson.

Remarks: Due to substantial differences in the allocation of ECTS-Credits in various curricula (Bachelor’s Programme Chemistry 2008 - Bachelor’s Programme Chemistry 2023), the requirements for this course vary. Information will be provided by the instructor at the beginning of the course.